HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18373524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18373479 | HCID 18373479 | — |
| Product | HCID 18373524 | HCID 18373524 | 33.3% |
Reaction Steps
Following the general hydrolysis procedure outlined in example 15, N-(4-pyridinyl)-2,6-dichloro-3-nitrobenzenesulfonamide (540 mg, 1.55 mmol), 80% NaH (217 mg,7.25 mmol) and water (0.045mL, 2.46 mmol) were reacted to form the desired product (170 mg, 33%). EI-MS m/z 328(M-H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-062d8fa13c8a4951af89bb46f2e980f8 |
| Source note | uspto-grants-2002_12 |