HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53826154, compound → HCID 53930485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53826154 | HCID 53826154 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 53930485 | HCID 53930485 | 91% |
Reaction Steps
Following the general hydrogenation procedure outlined in example 15, (N-cyclopentyl)-6-chloro-2-hydroxy-3-nitrobenzenesulfonamide (0.54 g, 1.7 mmol) was reduced with hydrogen and 10%,Pd/C (0.54 g) to form the desired product (0.45 g, crude). LC-MS m/z 291(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-32ddba358c9140f78add32affe316e94 |
| Source note | uspto-grants-2002_12 |