HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 18373570, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | Chlorophenyl isocyanate | HCID 76833 | — |
| Reactant | HCID 53930485 | HCID 53930485 | — |
| Product | HCID 18373570 | HCID 18373570 | 43.3% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, (N-cyclopentyl)-3-amino-6-chloro-2-hydroxybenzenesulfonamide (0. 15 g, 0.52 mmol) and 2-chlorophenylisocyanate (62 μL, 0.52 mmol) were coupled to form the desired urea (0.1 g, 43%). LC-MS n/z 444(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-f6e7944131a24f3e9fd1fd7b4e013c37 |
| Source note | uspto-grants-2002_12 |