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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2301635Generated: October 31, 2026

Water → HCID 18373494, compound

https://huagongshe.com/reaction/2301635

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium hydrideHCID 24758—
ReactantHCID 17927806HCID 17927806—
ProductHCID 18373494HCID 18373494—

Reaction Steps

Following the general hydrolysis procedure outlined in example 15, N-(2-isopropoxyethyl)-2,6-dichloro-3-nitrobenzenesulfonamide (1.635 g, 4.58 mmol), 60% NaH (0.41 g, 13.74 mmol) and water (0.099 mL, 5.50 mmol) were reacted. The crude product (1.676 g) was carried on to the next step without purification. LC-MS (m/z) 340 (M-H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06500863B1
Source datasetuspto-grants-2002_12
ORD IDord-b6b8ab4a977d4a9281d8b2370661fc9c
Source noteuspto-grants-2002_12