HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18373452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 17927853 | HCID 17927853 | — |
| Product | HCID 18373452 | HCID 18373452 | — |
Reaction Steps
Following the general hydrolysis procedure outlined in example 15, N-(2-ethoxyethyl)-2,6-dichloro-3-nitrobenzenesulfonamide (1.78 g, 5.16 mmol), 80% NaH (0.46 g, 15.48mmol) and water (111 μL, 6.20mmol) were reacted. The crude product (1.63 g) was carried onto the next step without purification. LC-MS (m/z) 325.0(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-cbfa3feee9eb45ceb31aa931910e19ba |
| Source note | uspto-grants-2002_12 |