HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 17927834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Dichloro-3-nitrobenzene-1-sulfonyl chloride | HCID 23447772 | — |
| Product | HCID 17927834 | HCID 17927834 | 75% |
Reaction Steps
Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (2.0 g, 6.88 mmol), tert-butylamine (503 mg, 6.88mmol) and triethylamine(l.43 mL, 10.32 mmol) were reacted to form the desired product (1.67 g, 75%). 1H NMR (MeOD-d4): δ 7.91 (d, 1H), 7.78 (d, 1H), 1.25 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-30d41e327aab4db4a99b7e1c1da1b2f2 |
| Source note | uspto-grants-2002_12 |