Water → HCID 18373434, compound

Participants

Reaction Steps

Following the general hydrolysis procedure outlined in example 15, N-(tert-butyl)-2,6-dichloro-3-nitrobenzenesulfonamide (1.67 g, 5.1 mmol), 60% NaH (612 mg, 15.3 mmol) and water (92 μL, 5l mmol) were reacted to form the crude product (1.54 g), which was carried on to the next step without purification. 1H NMR (MeOD-d4): δ 8.00 (d, 1H), 7.08 (d, 1H), 1.24 (s, 9H).

Provenance & Evidence