HCID 18373434, compound → HCID 18373538, compound

Participants

Reaction Steps

Following the general hydrogenation procedure outlined in example 15, crude N-(tert-butyl)6chloro-2-hydroxy-3-nitrobenzenesulfonamide (1 .54 g) was reduced with hydrogen and 10% Pd/C (670 mg). The crude product (1.23 g) was carried on to the next step without purification. 1H NMR (MeOD-d4): 8 6.82 (m, 2H), 1.22 (s, 9H).

Provenance & Evidence