HCID 17927863, compound → HCID 18373472, compound

Participants

Reaction Steps

Following the general hydrogenation procedure outlined in example 15, 6-chloro-1-(1,1 -dioxidothiomorpholinosulfonyl)-2-hydroxy-3-nitrobenzene (220 mg, 0.60 mmol) was reduced with hydrogen and 10% Pd/C (100 mg) to give the desired (186 mg, 92%). 1H NMR (MeOD-d4): δ 6.88 (m, 2H), 3.85 (t, 4H), 3.22 (t, 4H).

Provenance & Evidence