HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 53987021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 1,2-Dichloro-3-isocyanatobenzene | HCID 33050 | — |
| Reactant | HCID 18373472 | HCID 18373472 | — |
| Product | HCID 53987021 | HCID 53987021 | 34% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, 4-chloro-3-(1,1-dioxidothiomorpholinosulfonyl)-2-hydroxyaniline (62 mg, 0.18 mmol) and 2,3-dichlorophenylisocyanate (41 mg, 0.22 mmol) were coupled to form the desired urea (32 mg, 34%). LC-MS (m/z) 528.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b8f310574a05438a8d670dc6fca58bc3 |
| Source note | uspto-grants-2002_12 |