HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 18373446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | HCID 18373472 | HCID 18373472 | — |
| Product | HCID 18373446 | HCID 18373446 | 29% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, 4-chloro-3-(1,1-dioxidothiomorpholinosulfonyl)-2-hydroxyaniline (62 mg, 0.18 mmol) and 2-bromophenylisocyanate (44 mg, 0.22 mmol) were coupled to form the desired urea (28 mg, 29%). LC-MS (m/z) 539.8 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a7097f57b78c433e900fafc3648da241 |
| Source note | uspto-grants-2002_12 |