HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18373469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Aminomethyl-1-ethylpyrrolidine | HCID 117295 | — |
| Reactant | 2,6-Dichloro-3-nitrobenzene-1-sulfonyl chloride | HCID 23447772 | — |
| Product | HCID 18373469 | HCID 18373469 | — |
Reaction Steps
Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (2.0 g, 6.88 mmol), 2-aminomethyl- 1-ethyl-pyrolidine (882 mg, 6.88 mmol) and triethylamine(1.92 mL, 13.76 mmol) were reacted. The crude product (2.64 g) was carried on to the next step without purification. LC-MS (m/z) 382.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-972e8c10cea74f21a2152b6f3f10f251 |
| Source note | uspto-grants-2002_12 |