Phthalic Anhydride → 2-[2,6-di(propan-2-yl)phenyl]isoindole-1,3-dione

HRID 2301916Notes

Reaction equation

HRID 2301916 reaction equation
[C:1]1(=[O:11])[O:6][C:4](=O)[C:3]2=[CH:7][CH:8]=[CH:9][CH:10]=[C:2]12.[CH:12]([C:15]1[CH:21]=[CH:20][CH:19]=[C:18]([CH:22]([CH3:24])[CH3:23])[C:16]=1[NH2:17])([CH3:14])[CH3:13]>>[CH:22]([C:18]1[CH:19]=[CH:20][CH:21]=[C:15]([CH:12]([CH3:14])[CH3:13])[C:16]=1[N:17]1[C:1](=[O:11])[C:2]2=[CH:10][CH:9]=[CH:8][CH:7]=[C:3]2[C:4]1=[O:6])([CH3:24])[CH3:23]

Participants

3

Reactant 2

HCID 6811Phthalic AnhydrideHCID 32484Diisopropylaniline

Product 1

HCID 99953752-[2,6-di(propan-2-yl)phenyl]isoindole-1,3-dione

Procedure

7.41 g of phthalic anhydride and 8.86 g of 2,6-diisopropylaniline were mixed, and reacted at a temperature of 180° C. for 2 hours.

Workup

  1. customreacted at a temperature of 180° C. for 2 hours

Sources & evidence

ORD record
ord-4ad46f066a044dbd9ccf7a1fac5c4cad
Source dataset
uspto-grants-2002_08
Patent number
US06429212B1

Reaction notes

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