HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → N-(Tricyclo[4.3.1.1(3,8)]undec-3-yl)-2-quinoxalinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Quinoxaline-2-carbonyl chloride | HCID 2734681 | — |
| Reactant | Tricyclo[4.3.1.1~3,8~]undec-3-ylamine hydrochloride | HCID 22136454 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(Tricyclo[4.3.1.1(3,8)]undec-3-yl)-2-quinoxalinecarboxamide | HCID 22136388 | 57% |
Reaction Steps
Prepared from 2-quinoxaloyl chloride (135 mg, 0.70 mmol), tricyclo[4.3.1.1(3,8)]undec-3-ylamine hydrochloride (100 mg, 0.60 mmol), pyridine (5 mL), and water (50 mL) yielding 110 mg (57%) of (168):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06429207B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-c5ae2518cd2549b8ae4c7d7ed3f99f48 |
| Source note | uspto-grants-2002_08 |