HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromoindole → 5-Bromo-1-methyl-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromoindole | HCID 24905 | — |
| Reactant | 7-Bromoindole | HCID 2757020 | — |
| Reactant | 7-Bromo-1-methyl-1H-indole | HCID 21950069 | — |
| Product | 5-Bromo-1-methyl-1H-indole | HCID 285757 | — |
Reaction Steps
5-Bromo-1-methylindole was prepared from 5-bromoindole as described for the preparation of 7-bromo-1-methylindole from 7-bromoindole. Purification by chromatography using EtOAc:petroleum ether 1:10
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432962B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-11e7f7713be74a2c9c1624301c833944 |
| Source note | uspto-grants-2002_08 |