HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 53826-75-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 135854400 | HCID 135854400 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 53826-75-8 | HCID 135854401 | — |
Reaction Steps
A solution of the product from Example 12 (0.9 g) and bromine (0.3 ml) in glacial acetic acid (100 ml) were heated at 100° C. for 2 hours. On cooling the solvent was removed and the residue was dried. The residue was recrystallised from acetic acid to give the title product, m.p. 226-229° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432964B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-8e00d609f350423d8533d2fd13a160bf |
| Source note | uspto-grants-2002_08 |