HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloro-5,6-dicyano-1,4-benzoquinone → HCID 70103175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloro-5,6-dicyano-1,4-benzoquinone | HCID 6775 | — |
| Reactant | HCID 9901595 | HCID 9901595 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | HCID 70103175 | HCID 70103175 | — |
Reaction Steps
A solution of 3-(2-Amino-ethyl)-6-benzyl-1,6,7,8-tetrahydro-pyrrolo[2,3-g]isoquinolin-5-one (1 mmole) and 2,3-dichloro-5,6-dicyanobenzoquinone (2 mmole) in chlorobenzene (15 mL) at reflux under nitrogen for 24 hours provides the titled compound as a yellow colored solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432974B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-f97842e6764f4cf6af3032bed6872399 |
| Source note | uspto-grants-2002_08 |