HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18461100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | Trimethylsilyl iodide | HCID 85247 | — |
| Reactant | HCID 22958908 | HCID 22958908 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 18461100 | HCID 18461100 | — |
Reaction Steps
A solution of the 3-benzyl-6-(tetrahydro-pyran-2-yloxy)-8-aza-bicyclo[3.2.1]octane-8-carboxylic acid ethyl ester and 0.5 mL of trimethylsilyl iodide in 25 mL of chloroform was kept at room temperature for 48 h, shaken with 25 mL of 6N NaOH and dilute sodium sulfite and dried over magnesium sulfate. Removal of solvents gave 0.2 g of a resin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432976B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-938313be508d4345beaefbe01d0dc735 |
| Source note | uspto-grants-2002_08 |