HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 18626419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 18626421 | HCID 18626421 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18626419 | HCID 18626419 | — |
Reaction Steps
The product of Step 3 (183 mg) was dissolved in 5 ml of acetic acid. The solution was hydrogenated over 25 hours at atmospheric pressure in the presence of 10 mg of 10% Pd/C. The mixture was filtered and the filtrate was concentrated in vacuo to give the product. FAB ms: C20H20N3F:321; Observed: 322 (M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432980B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-8a09144e83d94fb4871cd38191db537b |
| Source note | uspto-grants-2002_08 |