HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 18461151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 1-(2-Chloroethyl)piperidine | HCID 74827 | — |
| Reactant | HCID 18461165 | HCID 18461165 | — |
| Product | HCID 18461151 | HCID 18461151 | 81.4% |
Reaction Steps
1.6 g of the title compound was prepared from 1.45 g (3.49 mmol) of [2-(4-methoxyphenyl)-6-methoxybenzo[b]thien-3-yl][3-cyano-4-hydroxyphenyl]methanone, 1.3 g(7 mmol) of 1-(2-chloroethyl)piperidine, and 4.9 g (15 mmol) of Cs2CO3 in a manner similar to that in Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432982B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b4bfbcea142c49b8a7d5f53e7a4864db |
| Source note | uspto-grants-2002_08 |