4-Hydroxybenzaldehyde → HCID 86587893, compound

HRID 2303529Notes

Reaction equation

HRID 2303529 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.I[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17].[CH3:18][C:19]([N+:22]([O-])=[O:23])([CH3:21])[CH3:20]>>[CH2:11]([O:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[N+:22]([C:19]([CH3:21])([CH3:20])[CH3:18])[O-:23])=[CH:4][CH:3]=1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]

Participants

4

Reactant 3

HCID 1264-HydroxybenzaldehydeHCID 116722-Methyl-2-nitropropaneHCID 202741-Iodoheptane

Product 1

HCID 86587893HCID 86587893, compound

Procedure

The title compound was prepared according to the procedure described in Example 2 using 4-hydroxybenzaldehyde, 1-iodoheptane and 2-methyl-2-nitropropane. The title compound was isolated in 60% overall yield as a solid, m.p. 68.5° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-6a9fc559c83a4d2e97ce12292ad278fa
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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