HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 86587906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Reactant | 2-Fluoro-4-hydroxybenzonitrile | HCID 2734675 | — |
| Product | HCID 86587906 | HCID 86587906 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 29 using 2-fluoro-4-hydroxybenzonitrile, ethyl iodide and N-tert-butylhydroxylamine. The title compound was isolated in 64.7% overall yield as slightly yellowish crystals. m.p. 82.5° C. (Rf=0.16 on a silica gel plate using hexanes/ethyl acetate, 4:1, v:v, as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06433008B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-a367528e23a846f38674a56b75b906c2 |
| Source note | uspto-grants-2002_08 |