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HRID2303572

反应详情

EQUATION

反应方程式

HRID 2303572 的结构方程式

REACTANTS

反应物

3
结构：CNC
HCID674

Dimethylamine

C2H7N

结构：O
HCID962

Water

H2O

结构：CC(C)(C)NS(=O)(=O)c1cccc(S(=O)(=O)Cl)c1
HCID16793286

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)S(=O)(=O)c1cccc(S(=O)(=O)NC(C)(C)C)c1
HCID31679606

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Dimethylamine gas was allowed to bubble for 3 minutes into a solution of 1.8 grams (7 mmole) of 3-tert-butylsulfamoyl-benzenesulfonyl chloride in ethyl acetate. Water was added and the mixture was stirred at room temperature for 1 hour. The ethyl acetate layer was separated, dried over magnesium sulfate and concentrated in vacuo to a solid which was triturated with hexane/isopropyl ether to give 1.59 grams of the titled compound. m.p. 100-102° C.

WORKUP

后处理

  1. customThe ethyl acetate layer was separated
  2. dry with materialdried over magnesium sulfate
  3. concentrationconcentrated in vacuo to a solid which
  4. customwas triturated with hexane/isopropyl ether