HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → Benzene-1,3-disulfonic Acid Amide Tert-butyl Amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 3-Tert-butylsulfamoyl-benzenesulfonyl chloride | HCID 16793286 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Benzene-1,3-disulfonic Acid Amide Tert-butyl Amide | HCID 31065078 | — |
Reaction Steps
20 ml of concentrated ammonium hydroxide was added to a solution of 1 gram (3.2 mmole) 3-tert-butylsulfamoyl-benzenesulfonyl chloride in ethyl acetate. It was stirred vigorously for 8 hours. The ethyl acetate layer was separated dried over magnesium sulfate in vacuo to give 320 mg of the titled compound as a white solid. m.p. 151-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06433009B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-91517b4fe33b408d89b3bdb177ea7304 |
| Source note | uspto-grants-2002_08 |