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HRID2303573

反应详情

EQUATION

反应方程式

HRID 2303573 的结构方程式

REACTANTS

反应物

2
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：CC(C)(C)NS(=O)(=O)c1cccc(S(=O)(=O)Cl)c1
HCID16793286

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)NS(=O)(=O)c1cccc(S(N)(=O)=O)c1
HCID31065078

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

20 ml of concentrated ammonium hydroxide was added to a solution of 1 gram (3.2 mmole) 3-tert-butylsulfamoyl-benzenesulfonyl chloride in ethyl acetate. It was stirred vigorously for 8 hours. The ethyl acetate layer was separated dried over magnesium sulfate in vacuo to give 320 mg of the titled compound as a white solid. m.p. 151-154° C.

WORKUP

后处理

  1. customThe ethyl acetate layer was separated
  2. dry with materialdried over magnesium sulfate in vacuo