HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10165687, compound → HCID 88008002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10165687 | HCID 10165687 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 88008002 | HCID 88008002 | 196.9% |
Reaction Steps
Using 2.54 g of 5-{4-[6-(2-chloro-4-hydroxy-3,5-dimethylphenoxy)-1-methyl-1H-benzimidazol-2-ylmethoxy]benzyl}thiazolidine-2,4-dione and 50 ml of a 4N hydrochloric acid/ethyl acetate solution, reaction and purification were carried out in a similar manner to that described in Example (2-2b), whereby 2.67 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-f0e53350d6ff49a2aeff9003fe20265b |
| Source note | uspto-grants-2002_08 |