HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461431, compound → HCID 86758427, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461431 | HCID 18461431 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 86758427 | HCID 86758427 | — |
Reaction Steps
A mixture of t-butyl N-{2-[4-(2,4-dioxothiazolidin-5-ylmethyl)phenoxyacetylamino]-5-[3-(morpholin-4-yl)phenoxy]phenyl)-N-methylcarbamate and 20 ml of 4N hydrochloric acid/dioxane was stirred at room temperature for 3 hours. The reaction mixture was evaporated to dryness under reduced pressure, followed by the addition of ether. The insoluble product was collected by filtration and washed with ether, whereby 1.27 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-34650a43780042b390e542ad0fb04735 |
| Source note | uspto-grants-2002_08 |