HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461336, compound → HCID 77844928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461336 | HCID 18461336 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 77844928 | HCID 77844928 | 92% |
Reaction Steps
In a similar manner to that described in Example (2-2a), a reaction was carried out using t-butyl N-{2-[4-(2,4-dioxothiazolidin-5-ylmethyl)phenoxyacetylamino]-5-[2-(pyrrolidin-1-yl)phenoxy]phenyl}-N-methylcarbamate (1.25 g) and 4N hydrogen chloride/dioxane (25 ml) and the reaction mixture was purified to give the title compound (0.94 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-8bf61149e27340d3aad3eca0bf7482c6 |
| Source note | uspto-grants-2002_08 |