HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461417, compound → HCID 18461288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461417 | HCID 18461417 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461288 | HCID 18461288 | 93.7% |
Reaction Steps
By using 3.12 g of t-butyl N-[5-(4-methoxymethoxy-3,5-dimethylphenoxy)-2-nitrophenyl]-N-methylcarbamate, 0.33 g of 10% palladium on carbon and 30 ml of methanol, reaction and purification were carried out in a similar manner to that described in Reference Example 7, whereby 2.72 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-03bb081ff89e41d4bf68d88105d108d1 |
| Source note | uspto-grants-2002_08 |