HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 18461440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 18461357 | HCID 18461357 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18461440 | HCID 18461440 | 96.8% |
Reaction Steps
By using 5.0 g of t-butyl N-{5-[3-(morpholin-4-yl)phenoxy]-2-nitrophenyl}-N-methylcarbamate, 0.5 g of 10% palladium on carbon and a mixed solvent of 30 ml of methanol and 70 ml of toluene, reaction and purification were carried out in a similar manner to that described in Reference Example 7, whereby 4.5 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-0b8ba4a62bdb45c894b4acddc0a696e4 |
| Source note | uspto-grants-2002_08 |