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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303859Generated: November 3, 2026

Methanol → HCID 18461440, compound

https://huagongshe.com/reaction/2303859

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 18461357HCID 18461357—
CatalystPalladiumHCID 23938—
SolventTolueneHCID 1140—
ProductHCID 18461440HCID 1846144096.8%

Reaction Steps

By using 5.0 g of t-butyl N-{5-[3-(morpholin-4-yl)phenoxy]-2-nitrophenyl}-N-methylcarbamate, 0.5 g of 10% palladium on carbon and a mixed solvent of 30 ml of methanol and 70 ml of toluene, reaction and purification were carried out in a similar manner to that described in Reference Example 7, whereby 4.5 g of the title compound were obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-0b8ba4a62bdb45c894b4acddc0a696e4
Source noteuspto-grants-2002_08