HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461425, compound → HCID 18461459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461425 | HCID 18461425 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461459 | HCID 18461459 | 78.8% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-methyl-N-[2-nitro-5-(pyridine-2-ylthio)phenyl]carbamate (1.08 g), palladium on carbon (10%, 1.00 g) and methanol (20 ml) and the reaction mixture was purified to give the title compound (0.78 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b312bfcd63b84ccb9bd11e43bbcd1b18 |
| Source note | uspto-grants-2002_08 |