HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18184945, compound → HCID 18184998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18184945 | HCID 18184945 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18184998 | HCID 18184998 | 99.7% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-{5-[4-(1-adamantyl)phenoxy]-2-nitrophenyl}-N-methylcarbamate (4.28 g), palladium on carbon (10%, 0.42 g) and methanol (60 ml) and the reaction mixture was purified to give the title compound (4.00 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-80c2e5f759b64ebaa26bd9959c29e492 |
| Source note | uspto-grants-2002_08 |