HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461327, compound → HCID 18461433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461327 | HCID 18461327 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18461433 | HCID 18461433 | 69.9% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-{5-[4-(imidazole-1-yl)phenoxy]-2-nitrophenyl]-N-methylcarbamate (8.8 g), palladium on carbon (10%, 0.8 g) and N,N-dimethylformamide (160 ml) and the reaction mixture was purified to give the title compound (5.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-0beba9cf984e4e28aadd8a3fb762c356 |
| Source note | uspto-grants-2002_08 |