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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303885Generated: November 1, 2026

HCID 18461377, compound → HCID 18461266, compound

https://huagongshe.com/reaction/2303885

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18461377HCID 18461377—
CatalystPalladiumHCID 23938—
SolventToluene methanolHCID 21867641—
ProductHCID 18461266HCID 1846126689.5%

Reaction Steps

In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-methyl-N-[2-nitro-5-(2-phenylphenoxy)phenyl]carbamate (8.3 g), palladium on carbon (10%, 0.66 g) and toluene/methanol=7/3 (100 ml) and the reaction mixture was purified to give the title compound (6.9 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-0e91f33b60ff474db37343d1f07d7f3b
Source noteuspto-grants-2002_08