HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461377, compound → HCID 18461266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461377 | HCID 18461377 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Toluene methanol | HCID 21867641 | — |
| Product | HCID 18461266 | HCID 18461266 | 89.5% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-methyl-N-[2-nitro-5-(2-phenylphenoxy)phenyl]carbamate (8.3 g), palladium on carbon (10%, 0.66 g) and toluene/methanol=7/3 (100 ml) and the reaction mixture was purified to give the title compound (6.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-0e91f33b60ff474db37343d1f07d7f3b |
| Source note | uspto-grants-2002_08 |