HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461289, compound → HCID 18461481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461289 | HCID 18461289 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461481 | HCID 18461481 | 90.7% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-hydroxyphenylthio)-2-nitrophenyl]-N-methylcarbamate (2.84 g), palladium on carbon (10%, 1.52 g) and methanol (50 ml) and the reaction mixture was purified to give the title compound (2.37 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-de14aebf08bd4d51bd39af56c90fca93 |
| Source note | uspto-grants-2002_08 |