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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303892Generated: November 2, 2026

HCID 18461263, compound → HCID 18461269, compound

https://huagongshe.com/reaction/2303892

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18461263HCID 18461263—
ReactantToluene ethylacetateHCID 21584019—
CatalystPalladiumHCID 23938—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 18461269HCID 1846126997.6%

Reaction Steps

In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[2-nitro-5-(4-phenylphenoxy)phenyl]-N-methylcarbamate (5.32 g), palladium on carbon (10%, 0.68 g) and toluene/ethyl acetate=1/1 (140 ml) and the reaction mixture was purified to give the title compound (4.82 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-30f84e1bb2eb447a9d6b6dc412ef8686
Source noteuspto-grants-2002_08