HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461263, compound → HCID 18461269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461263 | HCID 18461263 | — |
| Reactant | Toluene ethylacetate | HCID 21584019 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 18461269 | HCID 18461269 | 97.6% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[2-nitro-5-(4-phenylphenoxy)phenyl]-N-methylcarbamate (5.32 g), palladium on carbon (10%, 0.68 g) and toluene/ethyl acetate=1/1 (140 ml) and the reaction mixture was purified to give the title compound (4.82 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-30f84e1bb2eb447a9d6b6dc412ef8686 |
| Source note | uspto-grants-2002_08 |