HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461307, compound → HCID 18461460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461307 | HCID 18461307 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461460 | HCID 18461460 | 101.3% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-hydroxy-3,5-di-t-butylphenoxy)-2-nitrophenyl]-N-methylcarbamate (0.58 g), palladium on carbon (10%, 0.12 g) and methanol (20 ml) and the reaction mixture was purified to give the title compound (0.55 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-794b02fc555a4d679b038114f0c16cc9 |
| Source note | uspto-grants-2002_08 |