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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303903Generated: October 31, 2026

HCID 131723435, compound → HCID 131723432, compound

https://huagongshe.com/reaction/2303903

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131723435HCID 131723435—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 131723432HCID 13172343283.4%

Reaction Steps

In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-methyl-N-[5-(4-methylthiophenoxy)-2-nitrophenyl]carbamate (2.53 g), palladium on carbon (10%, 2.5 g) and methanol (55 ml) and the reaction mixture was purified to give the title compound (1.94 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-2b0dfaa2d6e647729854c0f3f83df705
Source noteuspto-grants-2002_08