HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131723435, compound → HCID 131723432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131723435 | HCID 131723435 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131723432 | HCID 131723432 | 83.4% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-methyl-N-[5-(4-methylthiophenoxy)-2-nitrophenyl]carbamate (2.53 g), palladium on carbon (10%, 2.5 g) and methanol (55 ml) and the reaction mixture was purified to give the title compound (1.94 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-2b0dfaa2d6e647729854c0f3f83df705 |
| Source note | uspto-grants-2002_08 |