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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303906Generated: October 30, 2026

HCID 18461309, compound → HCID 18461251, compound

https://huagongshe.com/reaction/2303906

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18461309HCID 18461309—
ReactantToluene ethylacetateHCID 21584019—
CatalystPalladiumHCID 23938—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 18461251HCID 1846125188.9%

Reaction Steps

In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-benzylphenoxy)-2-nitrophenyl]-N-methylcarbamate (12.2 g), palladium on carbon (10%, 0.91 g) and toluene/ethyl acetate=1/1 (140 ml) and the reaction mixture was purified to give the title compound (10.1 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-3682f9670cbf4696a62979b594321018
Source noteuspto-grants-2002_08