HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461410, compound → HCID 18461361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461410 | HCID 18461410 | — |
| Reactant | Toluene ethylacetate | HCID 21584019 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 18461361 | HCID 18461361 | 83.9% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(3-hydroxyphenoxy)-2-nitrophenyl]-N-methylcarbamate (7.8 g), palladium on carbon (10%, 0.9 g) and toluene/ethyl acetate=1/1 (140 ml) and the reaction mixture was purified to give the title compound (6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-37f815c6f49e443eb6c96e12d23bde81 |
| Source note | uspto-grants-2002_08 |