HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461285, compound → HCID 18461424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461285 | HCID 18461285 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18461424 | HCID 18461424 | 74.9% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-methyl-N-{2-nitro-5-[4-(2-triphenylmethyltetrazol-5-yl)phenoxy]phenyl}carbamate (0.98 g), palladium on carbon (10%, 0.13 g) and ethyl acetate (100 ml) and the reaction mixture was purified to give the title compound (0.70 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-3fdd12fcd4954ea1adaecde44fdc6449 |
| Source note | uspto-grants-2002_08 |