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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303914Generated: November 2, 2026

Hydrochloric Acid → HCID 18461445, compound

https://huagongshe.com/reaction/2303914

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantPotassium HydroxideHCID 14797—
ReactantHCID 18461312HCID 18461312—
SolventMethanolHCID 887—
ProductHCID 18461445HCID 1846144599.6%

Reaction Steps

To a solution of potassium hydroxide (1.51 g) in methanol (12 ml) was added 4-benzyloxy-2,5-di-t-butylphenyl acetate (4.9 g). The mixture was allowed to stand at ambient temperature overnight. The reaction mixture was neutralized with dilute hydrochloric acid and then extracted with ethyl acetate. The ethyl acetate solution was dried over anhydrous sodium sulfate and evaporated to dryness to give the title compound (4.3 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-ccba7ba01f2b4a9eba7f73a10f0c23e5
Source noteuspto-grants-2002_08