HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18461445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 18461312 | HCID 18461312 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18461445 | HCID 18461445 | 99.6% |
Reaction Steps
To a solution of potassium hydroxide (1.51 g) in methanol (12 ml) was added 4-benzyloxy-2,5-di-t-butylphenyl acetate (4.9 g). The mixture was allowed to stand at ambient temperature overnight. The reaction mixture was neutralized with dilute hydrochloric acid and then extracted with ethyl acetate. The ethyl acetate solution was dried over anhydrous sodium sulfate and evaporated to dryness to give the title compound (4.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-ccba7ba01f2b4a9eba7f73a10f0c23e5 |
| Source note | uspto-grants-2002_08 |