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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2303916Generated: November 1, 2026

HCID 18461310, compound → HCID 18461278, compound

https://huagongshe.com/reaction/2303916

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18461310HCID 18461310—
CatalystPalladiumHCID 23938—
SolventHCID 22505858HCID 22505858—
ProductHCID 18461278HCID 1846127863.7%

Reaction Steps

In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-benzyloxy-2,5-di-t-butylphenoxy)-2-nitrophenyl]-N-methylcarbamate (7.1 g), palladium on carbon (10%, 0.7 g) and toluene/methanol/ethyl acetate=16/16/25 (57 ml) and the reaction mixture was purified to give the title compound (3.56 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06432993B1
Source datasetuspto-grants-2002_08
ORD IDord-e7a44437700d401d9ba7815bdf2d2472
Source noteuspto-grants-2002_08