HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18461310, compound → HCID 18461278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18461310 | HCID 18461310 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | HCID 22505858 | HCID 22505858 | — |
| Product | HCID 18461278 | HCID 18461278 | 63.7% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-[5-(4-benzyloxy-2,5-di-t-butylphenoxy)-2-nitrophenyl]-N-methylcarbamate (7.1 g), palladium on carbon (10%, 0.7 g) and toluene/methanol/ethyl acetate=16/16/25 (57 ml) and the reaction mixture was purified to give the title compound (3.56 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-e7a44437700d401d9ba7815bdf2d2472 |
| Source note | uspto-grants-2002_08 |