HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18537656, compound → HCID 18537692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18537656 | HCID 18537656 | — |
| Reactant | Toluene ethylacetate | HCID 21584019 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 18537692 | HCID 18537692 | 100.5% |
Reaction Steps
In a similar manner to that described in Reference Example 7, a reaction was carried out using t-butyl N-{5-[4-(t-butoxycarbonyl-n-hexylamino)phenoxy]-2-nitrophenyl}-N-methylcarbamate (13.8 g), palladium on carbon (10%, 1.0 g) and toluene/ethyl acetate=1/1 (140 ml) and the reaction mixture was purified to give the title compound (13.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432993B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b5ee701cd8fd409698e6883bcc8c06de |
| Source note | uspto-grants-2002_08 |