Allyl glycidyl ether → HCID 131723438, compound

Participants

Reaction Steps

10.0 g (54.7 mmol) of lysine monohydrochloride and a 31.8% NaOH solution (5.0 g of deionized water/8.75 g 50% NaOH) are placed into a round-bottomed flask equipped with a stirrer, nitrogen inlet and a thermoregulator. This mixture is heated with stirring. When a temperature of 650° C. is reached, 6.25 g (54.7 mmol) allyl glycidyl ether (AGE) is added over a one hour period. The reaction mixture is then stirred for two hours at 65° C., after which time the reaction is complete as determined by gas chromatography. This product is obtained as a clear yellow solution of 62.5% solids by weight.

Provenance & Evidence