HCID 12020528, compound → HCID 12020532, compound

Participants

Reaction Steps

In similar manners to those described for the synthesis of sulfamate 11a, compound 11g was prepared from compound 8. FAB-MS m/z 405 (M+H)+; 1H NMR (270 MHz, DMSO-d6) δ 0.91 (s, 3H, CH3), 1.03 (t, 3H, J=7.1 Hz, CH2CH3), 3.12 (m, 2H, CH2CH3), 6.36 (s, 1H, 16-CH), 6.97 (d, 1H, J=2.3 Hz, ArH), 7.01 (dd, 1H, J=2.3, 8.6 Hz, ArH), 7.33 (d, 1H, J=8.6 Hz, ArH), 7.75 (t, 1H, J=5.7 Hz, NHCH2), 7.89 (s, 2H, NH2).

Provenance & Evidence