HCID 12019228, compound → HCID 12019232, compound

Participants

Reaction Steps

In similar manners to those described for the synthesis of compound 7, compound 29d was prepared from compound 11d. TOF-MS m/z 435 (M+H)+; 1H NMR (270 MHz, DMSO-d6) δ 0.60 (s, 3H, CH3), 0.84 (d, 6H, J=6.9 Hz, CH(CH3)2), 2.60-3.16 (m, 2H, NHCH2), 6.95 (d, 1H, J=2.3 Hz, ArH), 7.00 (dd, 1H, J=2.3, 8.6 Hz, ArH), 7.34 (d, 1H, J=8.6 Hz, ArH), 7.49 (brt, 1H, J=5.6 Hz, NHCH2), 7.84 (brs, 2H, NH2).

Provenance & Evidence