Hydrochloric Acid → HCID 9885320, compound

Participants

Reaction Steps

The procedure of Example 1 was followed starting with (C) of Example 1 (2.0 g, 6.4 mmol) and using piperidine in place of dibutylamine to produce 1.1 g, (41% yield) of the named compound as the HCl salt, mp 127°-128° C. IR(KBr): 3400,1600 cm−1. MS: 363(MH+). 1H NMR (CD3 OD): δ 7.89-6.81 (m, 10H), 4.24 (t, J=5.5 Hz, 2H), 2.65 (m, 6H), 1.75 (m, 8H).

Provenance & Evidence