Thionyl Chloride → HCID 15294258, compound

HRID 2304696Notes

Reaction equation

HRID 2304696 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[CH:14]([CH3:16])[CH3:15])[C:8](O)=[O:9])(=[O:4])=[O:3].S(Cl)([Cl:19])=O>CN(C=O)C.C1(C)C=CC=CC=1>[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[CH:14]([CH3:16])[CH3:15])[C:8]([Cl:19])=[O:9])(=[O:4])=[O:3]

Participants

5

Reactant 2

HCID 24386Thionyl ChlorideHCID 106339154-Isopropyl-3-methylsulfonylbenzoic acid

Product 1

HCID 15294258HCID 15294258, compound

Reagents, catalysts & solvents 2

HCID 6228DimethylformamideCatalystHCID 1140TolueneSolvent

Procedure

4.0 g of 3-methylsulfonyl-4-i-propylbenzoic acid, 1.5 ml of thionyl chloride and 3 drops of DMF are heated under reflux for 10 h in 30 ml of toluene. The solvent is subsequently removed in vacuo and the product is taken for further use without purification.

Workup

  1. customThe solvent is subsequently removed in vacuo
  2. customthe product is taken for further use without purification

Sources & evidence

ORD record
ord-5ac7cbcc99134cc1a6ba255928245732
Source dataset
uspto-grants-2002_08
Patent number
US06436999B1

Reaction notes

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