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HRID2304696

反应详情

EQUATION

反应方程式

HRID 2304696 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CC(C)c1ccc(C(=O)O)cc1S(C)(=O)=O
HCID10633915

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)c1ccc(C(=O)Cl)cc1S(C)(=O)=O
HCID15294258

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CN(C)C=O
催化剂HCID6228

N,N-Dimethylformamide

C3H7NO

结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

4.0 g of 3-methylsulfonyl-4-i-propylbenzoic acid, 1.5 ml of thionyl chloride and 3 drops of DMF are heated under reflux for 10 h in 30 ml of toluene. The solvent is subsequently removed in vacuo and the product is taken for further use without purification.

WORKUP

后处理

  1. customThe solvent is subsequently removed in vacuo
  2. customthe product is taken for further use without purification