HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18459276, compound → HCID 9806181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18459276 | HCID 18459276 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 9806181 | HCID 9806181 | — |
Reaction Steps
A mixture of N-benzyloxy-2-hydroxy-2-[(4-methoxybenzenesulfonyl)methyl]-3-(4-phenylbenzenesulfonyl)-propionamide (0.152 g), 10% palladium on carbon, and 50 mL of absolute ethanol is placed under 20 psi of hydrogen, and agitated overnight at ambient temperature. The mixture is filtered through a Celite pad, rinsing with ethanol and with ethyl acetate. Concentration of the filtrate affords the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06437177B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-60ee97177b0945e7a78f1a0bab94a0e2 |
| Source note | uspto-grants-2002_08 |